| 引用本文:芮海波1，赵学龙1，王文晓2，张国花2.HPLC法对杏桔合剂中桔梗皂苷D的含量测定研究[J].世界中医药,2015,10(06):. |
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| HPLC法对杏桔合剂中桔梗皂苷D的含量测定研究 |
| HPLC Method for Determination of Platycodin D in Apricot Orange Mixture |
| 投稿时间：2014-06-16 |
| DOI：10.3969/j.issn.1673-7202.2015.06.027 |
| 中文关键词: 杏桔合剂 桔梗皂苷D 含量 HPLC |
| English Keywords:Apricot orange mixture Platycodin D Content HPLC |
| 基金项目:南京市中医院青年科研基金课题（编号：2011YJ006） |
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| 中文摘要: |
| 目的:建立杏桔合剂中桔梗皂苷D的含量测定方法，为杏桔合剂的质量控制提供量化参考。方法：采用HPLC方法测定桔梗皂苷D的含量。结果：桔梗皂苷D在0.5～8 μg范围内线性关系良好，回归方程:y=238632x+10382，r=0.9997，加样回收率93.64%，RSD=1.54%。结论：应用HPLC测定杏桔合剂中桔梗皂苷D含量的方法可行，可以作为其质量控制的参考依据。 |
| English Summary: |
| To establish content determination method of platycodin D in apricot orange mixture so as to provide quantitative information for quality control of apricot orange mixture.Methods:HPLC was used to determine contents of platycodin D.Results:Platycodin D in the range 0.5 ~ 8ug had good linear relationship, and the regression equation was: y=238632x +10382, r=0.9997, recovery was 93.64%, RSD=1.54%.Conclusion:The method of HPLC to determine Platycodin D in apricot orange mixture is feasible, and it can be used as a reference for its quality control. |
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